1 All gas cylinders should be weighed and checked
against the gross mass which has been marked on the bottle. To allow
for difference of scales when check-weighing, a tolerance of 14 g
should be permitted. No gas cylinder should be fitted unless it has
passed one of the following two tests:
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.1 A storage period of at least 30 days after
filling. Weighing should take place before and after storage using
the same scales. There should be no loss of weight.
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.2 The leak test specified in paragraph 2.
2 This paragraph describes a leak test for CO2 cylinders
which is regarded as equivalent to weighing the filled cylinder before
and after at least 30 days of storage.
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.1 Materials required
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.1 Polythene bags of a suitable size to fit over
the head of the cylinder, e.g.:
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.1 for a 125 mm diameter cylinder the bag size
is approximately 230 mm open width x 300 mm length;
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.2 for a 100 mm diameter cylinder the bag size
is approximately 165 mm open width x 300 mm length; and
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.3 for a 90 mm diameter cylinder the bag size
is approximately 150 mm open width x 300 mm length.
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.2 Elastic bands of a suitable size.
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.3 A measuring glass, capacity 25 ml.
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.2 Test solution
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.1 The test liquid should be the standard test
solution used to indicate small amounts of CO2 gases (0.004N
sodium carbonate in a 2% weight/volume solution of phenolphthalein).
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.2 The solution should be stored in a cool place
in dark coloured glass bottles with a tight-fitting screw cap. The
shelf life should not exceed 12 months.
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.3 Method of testing
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.1 Lay the cylinder to be tested on its side in
a rack, such that the valve end is protruding. Make sure the valve
and shoulder of the cylinder are free from dust and other contaminants
by carefully wiping it with a clean, dry cloth. Remove the dust cap
to clean the valve, then replace the cap loosely.
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.2 Using the measuring glass, transfer 25 ml of
the test solution into a polythene bag.
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.3 Pass the open end of the bag over the valve
head and attach it to the cylinder body using one or more elastic
bands. Make sure there are no air gaps in the seal.
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.4 The polythene bag should hang 20 cm off the
valve end of the cylinder with the test solution in one corner.
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.5 Maintain the test for a period of not less
than one hour.
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.6 After the period of time stated in 2.3.5, shake
the solution gently and make the observations detailed in 2.4.
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.7 A control sample is necessary to detect any
contamination. The sample is made by pouring 25 ml of test solution
into a bag which is not fitted to a cylinder, but is sealed at the
open end with adhesive tape to exclude atmospheric contamination.
This bag should be placed on the rack in the vicinity of the cylinders
being tested.
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.4 Observations
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.1 A leak of carbon dioxide from the cylinder
will cause the pink colour of the test solution to fade. The test
solution will become clear as water.
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.2 If no colour change is observed, there is no
leak of gas from the cylinder.
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.3 The control sample should not change colour
during the test. If a colour change takes place, this indicates that
the atmosphere in the test area is contaminated with carbon dioxide
and tests carried out together with this control sample are invalid.
Tests should be repeated after corrective action has been taken on
the atmosphere.