A 50 cm3 sample of wax or bitumen should be placed
in a metal or glass cylindrical container, having a flat bottom, an
internal diameter of 55 mm and an internal height of 35 mm. The container,
without lid, should be placed in an automatically controlled electric,
constant ambient temperature oven with air circulation. The temperature
in the oven should be controlled at 16°C below the nominal release
temperature of the nozzle, but at not less than 50°C. The sample
should be weighed before and after 90 days exposure to determine any
loss of volatile matter. The sample should meet the requirements of 4.12.1.